›› 2007, Vol. 2 ›› Issue (3): 115-117.

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Structure determination of a C-19 steriod from the roots of Cynanchum amplexicaule

  

  • 收稿日期:2007-01-01 修回日期:2007-01-01 出版日期:2007-06-15 发布日期:2007-06-15

Structure determination of a C-19 steriod from the roots of Cynanchum amplexicaule

Huan Chen; Li Qiao, Yuzhi Zhou; Yao Yao; Jiaqing Cao; Huiming Hua; Yuehu Pei *   

  1. School of Traditional Chinese Materia Medica, Shenyang Pharmaceutical University, Shenyang 110016, China
  • Received:2007-01-01 Revised:2007-01-01 Online:2007-06-15 Published:2007-06-15
  • Contact: Yuehu Pei

Abstract: A C-19 steriod was isolated from the roots of Cynanchum amplexicaule (Sieb. et Zucc.) and its structure was established as 17-oxo-D-homo-1, 4, 6-androstatrien-3, 17-dione on the basis of spectral data. The complete assignment of its 1H and 13C NMR spectral signals was determined by 2D NMR spectral methods.

Key words: Cynanchum amplexicaule, 17-oxo-D-homo-1, 6-androstatrien-3, 17-dione, 2D NMR